Innovative in Situ Ball Mill for Xray Diffraction ...
The renewed interest of mechanochemistry as an ecofriendly synthetic route has inspired original methodologies to probe reactions, with the aim to rationalize unknown mechanisms. Recently, Friščić et al. (Nat. Chem. 2013, 5, 66−73, DOI: /) monitored the progress of milling reactions by synchrotron Xray powder diffraction (XRPD).